HCID 58548537, compound → HCID 58548620, compound

Participants

Reaction Steps

A solution of 2-(4-methoxy-cyclohexyl)-benzothiazole (1.2 g, 5.15 mmol) in HI (35%)(12 mL) was heated to 90° C. for 1 h. Then the reaction mixture was diluted with water (20 mL), extracted with EtOAc (2×) and the separated organic layer was washed with brine (2×), dried over Na2SO4, and concentrated to give the desired product (960 mg, 4.12 mmol, 85% yield) as brown solid.

Provenance & Evidence