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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1847119Generated: November 1, 2026

HCID 68008633, compound → HCID 68008765, compound

https://huagongshe.com/reaction/1847119

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68008633HCID 68008633—
CatalystHCID 178418390HCID 178418390—
SolventEthyl AcetateHCID 8857—
ProductHCID 68008765HCID 6800876576%

Reaction Steps

Compound 66 (3.7 mg, 0.0086 mmol) obtained in Example 68 was dissolved in ethyl acetate (2 mL), and 10% palladium-carbon (2.0 mg) was added thereto, followed by stirring at room temperature for 2 hours under a hydrgen atmosphere. The catalyst was sparated by filtration, followed by concentrating the filtrate to obtain the title compound (2.8 mg, 76%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08952003B2
Source datasetuspto-grants-2015_02
ORD IDord-f4008da15c9348799540003b382080bb
Source noteuspto-grants-2015_02