HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68008633, compound → HCID 68008765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68008633 | HCID 68008633 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68008765 | HCID 68008765 | 76% |
Reaction Steps
Compound 66 (3.7 mg, 0.0086 mmol) obtained in Example 68 was dissolved in ethyl acetate (2 mL), and 10% palladium-carbon (2.0 mg) was added thereto, followed by stirring at room temperature for 2 hours under a hydrgen atmosphere. The catalyst was sparated by filtration, followed by concentrating the filtrate to obtain the title compound (2.8 mg, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952003B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-f4008da15c9348799540003b382080bb |
| Source note | uspto-grants-2015_02 |