Ethyl Acetoacetate → HCID 178471719, compound

HRID 1847241Notes

Reaction equation

[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.[C:10]([O:16][CH2:17][CH3:18])(=[O:15])[CH2:11][C:12]([CH3:14])=[O:13]>>[CH2:17]([O:16][C:10](=[O:15])[C:11](=[C:6]([NH2:7])[C:5]1[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=1)[C:12](=[O:13])[CH3:14])[CH3:18]

Participants

Reactant 2

HCID 8868Ethyl Acetoacetate

HCID 121634-Chlorobenzonitrile

Product 1

HCID 178471719HCID 178471719, compound

Procedure

The title compound was synthesized in analogy to Example 1 from 4-chlorobenzonitrile and ethyl acetoacetate: MS (m/z) 268.2 (M+1).

Sources & evidence

ORD record: ord-475639ccbb7c4c2493c00ecddb77cc1d
Source dataset: uspto-grants-2015_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08952160B2

Reaction notes

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