Ethyl Acetoacetate → HCID 178471718, compound

HRID 1847263Notes

Reaction equation

[F:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[C:10]([O:16][CH2:17][CH3:18])(=[O:15])[CH2:11][C:12]([CH3:14])=[O:13]>>[CH2:17]([O:16][C:10](=[O:15])[C:11](=[C:4]([NH2:5])[C:3]1[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=1[F:1])[C:12](=[O:13])[CH3:14])[CH3:18]

Participants

Reactant 2

HCID 8868Ethyl Acetoacetate

HCID 678552-Fluorobenzonitrile

Product 1

HCID 178471718HCID 178471718, compound

Procedure

The title compound was synthesized in analogy to Example 1 from 2-fluoro-benzonitrile and ethyl acetoacetate: MS (m/z) 252.2 (M+1).

Sources & evidence

ORD record: ord-7dfd305e7c7147ffa9b24ad130867a3f
Source dataset: uspto-grants-2015_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08952160B2

Reaction notes

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