HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86681241, compound → HCID 86681247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86681241 | HCID 86681241 | — |
| Reactant | HCID 86681248 | HCID 86681248 | — |
| Product | HCID 86681247 | HCID 86681247 | — |
Reaction Steps
1-((2-(Methylthio)benzo[d]thiazol-6-yl)methyl)-1H-benzo[d]imidazole-5-carbonitrile was synthesized as a white solid (694 mg, 86%) using a procedure analogous to that described in Step 3 of Example 232, substituting N-(4-cyano-2-nitrophenyl)-N-((2-(methylthio)benzo[d]thiazol-6-yl)methyl)formamide from the previous step for N-(4-iodo-2-nitrophenyl)-N-((2-(methylthio)benzo[d]thiazol-6-yl)methyl)formamide used in Example 232. LCMS (ESI) m/z 337 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952058B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-136d2439f7f241d4bef5909c0d9a76c2 |
| Source note | uspto-grants-2015_02 |