HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 68613712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Acetyl-2-methylbenzoic acid | HCID 53435554 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68613712 | HCID 68613712 | — |
Reaction Steps
28 ml of dichloromethane, 4 ml of oxalyl chloride, and a drop of N,N-dimethylformamide were added to 5.0 g of 4-acetyl-2-methylbenzoic acid, and the mixture was stirred for 3 hours at room temperature. After removing the solvent by distilling under reduced pressure, 5.6 g of crude 4-acetyl-2-methylbenzyl chloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952175B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-7cc8f63a881b46209ee2126ddfb3cc6d |
| Source note | uspto-grants-2015_02 |