HCID 86673667, compound → HCID 86673671, compound

Participants

Reaction Steps

To a solution of methyl diazo dipentanoate 9 (27 mg, 0.086 mmol) in acetone (1 mL) was added dimethyldioxirane acetone solution (2.5 mL, ca. 0.07-0.09 M). The resulting mixture was stirred for 1 h and solvent and excess reagents were removed under reduced pressure to obtain 21 as bright yellow oil (yield=26 mg, quantitative).

Provenance & Evidence