HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyrrolidinemethanol, alpha,alpha-diphenyl-, (R)- → HCID 86706793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyrrolidinemethanol, alpha,alpha-diphenyl-, (R)- | HCID 7045371 | — |
| Reactant | (6-Hydroxy-2,3-dihydro-1-benzofuran-3-yl)acetic acid | HCID 23111800 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86706793 | HCID 86706793 | — |
Reaction Steps
A racemate (19 mg, 0.1 mmol) of (6-hydroxy-2,3-dihydro-1-benzofuran-3-yl)acetic acid was charged, methanol was added, and the racemate was dissolved. This solution and (R)-α,α-diphenyl-2-pyrrolidinemethanol (25.3 mg, 0.1 mmol) were mixed and stood. The precipitated crystals were collected by filtration to give the title compound. 9.9% de
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952185B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-56a460c301264808a294758634b608c3 |
| Source note | uspto-grants-2015_02 |