HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-(bicyclo[4.1.0]heptan-1-ylmethoxy)-5-chloro-2-fluorobenzoate → HCID 86703740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-(bicyclo[4.1.0]heptan-1-ylmethoxy)-5-chloro-2-fluorobenzoate | HCID 86703665 | — |
| Reactant | HCID 86703741 | HCID 86703741 | — |
| Product | HCID 86703740 | HCID 86703740 | — |
Reaction Steps
Following the procedure as described in Example 342 Step 4 and making variations as required to replace tert-butyl 4-(bicyclo[4.1.0]heptan-1-ylmethoxy)-5-chloro-2-fluorobenzoate with tert-butyl 5-chloro-4-((7,7-difluorobicyclo[4.1.0]heptan-3-yl)methoxy)-2-fluorobenzoate, the title compound was obtained as oil (0.35 g, 48%): MS (ES+) m/z 341.07 (M−55).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952169B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-186672c1bbd24c39b62e699dfd4452c9 |
| Source note | uspto-grants-2015_02 |