Methanesulfonamide → HCID 86703788, compound

Participants

Reaction Steps

The compound was prepared in a similar manner to step 2 of Example 412 from 4-(adamantan-1-ylmethoxy)-3-chloro-2,5-difluorobenzoic acid and methanesulfonamide. LCMS (Method D): RT=6.97 min, m/z: 434.1 [M+H]+. 1H NMR (400 MHz, DMSO-d6) δ 7.66 (dd, J=11.6, 6.6 Hz, 1H), 3.82 (d, J=2.0 Hz, 2H), 1.99 (s, 3H), 1.82-1.56 (m, 12H).

Provenance & Evidence