HCID 86703792, compound → HCID 86703791, compound

Participants

Reaction Steps

A solution of tert-butyl 5-chloro-4-((3,3-difluorocyclohexyl)methoxy)-2- fluorobenzoate (64.4 mg) in dichloromethane (0.34 mL) and trifluoroacetic acid (0.17 mL) was stirred at 0° C. for 10 min then at rt for 2 h. The contents were concentrated. The residue was re-dissolved with dichloromethane and concentrated. The crude was dried under vacuum and used directly.

Provenance & Evidence