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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1849999Generated: October 31, 2026

Sodium Hydroxide → HCID 131731332, compound

https://huagongshe.com/reaction/1849999

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 68750135HCID 68750135—
SolventWaterHCID 962—
SolventAcetonitrileHCID 6342—
ProductHCID 131731332HCID 131731332—

Reaction Steps

0.5 g (0.667 mmol) of the compound from example 9 is dissolved in 12.5 ml of acetonitrile and 62.5 ml of water, and 13 ml of 0.1N sodium hydroxide solution are added. After brief stirring, the mixture is lyophilized. After drying under high vacuum, 0.53 g (quant.) of the title compound remain.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08957017B2
Source datasetuspto-grants-2015_02
ORD IDord-e754481843f64ba9bc77b93c11e45d2e
Source noteuspto-grants-2015_02