HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 67469212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 58547489 | HCID 58547489 | — |
| Product | HCID 67469212 | HCID 67469212 | 100% |
Reaction Steps
To a solution of 4 N HCl/MeOH (10 mL) was added compound (13) (80 mg, 0.22 mmol) at 0° C. The resulting mixture was stirred at RT for 1 h. The mixture was concentrated under reduced pressure to give (14) (65 mg, yield 100%), which was used for the next step without further purification. ESI-MS (M+1): 258 calc. for C14H15N3O2 257.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957073B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-f389f51599c144dc9b0a3f3a894ec6af |
| Source note | uspto-grants-2015_02 |