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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1850247Generated: October 30, 2026

Hydrochloride methanol → HCID 67469212, compound

https://huagongshe.com/reaction/1850247

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloride methanolHCID 21893726—
ReactantHCID 58547489HCID 58547489—
ProductHCID 67469212HCID 67469212100%

Reaction Steps

To a solution of 4 N HCl/MeOH (10 mL) was added compound (13) (80 mg, 0.22 mmol) at 0° C. The resulting mixture was stirred at RT for 1 h. The mixture was concentrated under reduced pressure to give (14) (65 mg, yield 100%), which was used for the next step without further purification. ESI-MS (M+1): 258 calc. for C14H15N3O2 257.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08957073B2
Source datasetuspto-grants-2015_02
ORD IDord-f389f51599c144dc9b0a3f3a894ec6af
Source noteuspto-grants-2015_02