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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1850278Generated: October 31, 2026

Hydrochloride methanol → HCID 67468031, compound

https://huagongshe.com/reaction/1850278

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloride methanolHCID 21893726—
ReactantHCID 58547240HCID 58547240—
ProductHCID 67468031HCID 6746803198.8%

Reaction Steps

A solution of 3-(3-m-tolyl-quinoxalin-2-yl)-azetidine-1-carboxylic acid tert-butyl ester (69) (637 mg, 1.7 mmol) in 4N HCl/MeOH (25 mL) was stirred at RT for 30 min. The reaction mixture was concentrated to give 2-azetidin-3-yl-3-m-tolyl-quinoxaline hydrochloride (70) (523 mg, 1.68 mmol, yield 98.8%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08957073B2
Source datasetuspto-grants-2015_02
ORD IDord-bf3128f0f85643afa42a96af224f656a
Source noteuspto-grants-2015_02