HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-4-ethylbenzene → HCID 59484997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-4-ethylbenzene | HCID 15313 | — |
| Reactant | HCID 66760421 | HCID 66760421 | — |
| Product | HCID 59484997 | HCID 59484997 | 25% |
Reaction Steps
By using 1-(7-methoxy-2,2,4,6-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine (400 mg, 1.38 mmol) synthesized in Reference example 96 and 1-bromo-4-ethylbenzene (383 mg, 2.07 mmol), the reaction was carried out in the same manner as Reference example 59 to synthesize the title compound 133 mg (yield 25%). Melting point was 157 to 160° C. (hexane-ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957069B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-75442eca78854e77ab9918a40b699f70 |
| Source note | uspto-grants-2015_02 |