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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1850470Generated: October 30, 2026

1-Bromo-4-ethylbenzene → HCID 59484997, compound

https://huagongshe.com/reaction/1850470

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-4-ethylbenzeneHCID 15313—
ReactantHCID 66760421HCID 66760421—
ProductHCID 59484997HCID 5948499725%

Reaction Steps

By using 1-(7-methoxy-2,2,4,6-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine (400 mg, 1.38 mmol) synthesized in Reference example 96 and 1-bromo-4-ethylbenzene (383 mg, 2.07 mmol), the reaction was carried out in the same manner as Reference example 59 to synthesize the title compound 133 mg (yield 25%). Melting point was 157 to 160° C. (hexane-ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08957069B2
Source datasetuspto-grants-2015_02
ORD IDord-75442eca78854e77ab9918a40b699f70
Source noteuspto-grants-2015_02