HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1,3,4-thiadiazole → HCID 59485059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1,3,4-thiadiazole | HCID 2795198 | — |
| Reactant | 1-(2,4,6,7-Tetramethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine | HCID 66759810 | — |
| Product | HCID 59485059 | HCID 59485059 | 14% |
Reaction Steps
By using 1-(2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)piperazine (130 mg, 0.50 mmol) synthesized in Reference example 56 and 2-bromo-1,3,4-thiadiazole (165 mg, 1.0 mmol), the reaction was carried out in the same manner as Example 23 to synthesis the title compound 24 mg (yield 14%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957069B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-4c1f131429a4401696956c9a433fd721 |
| Source note | uspto-grants-2015_02 |