HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1851206Generated: October 31, 2026
N,N-Dimethylaniline → HCID 86630683, compound
https://huagongshe.com/reaction/1851206
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178432406 | HCID 178432406 | — |
| Product | HCID 86630683 | HCID 86630683 | — |
Reaction Steps
1.34 g of the product of step 1 were suspended in 20 mL POCl3. 1.06 mL N,N-dimethylaniline was added and the mixture was heated to 100° C. for 45 min. The excess of POCl3 was removed by distillation and the residue was treated with ice. The desired product precipitates and was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08957064B2 |
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| Source dataset | uspto-grants-2015_02 |
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| ORD ID | ord-d78e68c671a94f56b48a6248554837d6 |
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| Source note | uspto-grants-2015_02 |
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