HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178498471, compound → Methyl 5-amino-1H-pyrazole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178498471 | HCID 178498471 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 5-amino-1H-pyrazole-3-carboxylate | HCID 18445864 | — |
Reaction Steps
To 14.0 g methyl 3-nitro-1H-pyrazole-5-carboxylate in 200 mL methanol were added 1.2 g Pd/C (10% w/w). The mixture was stirred under H2-atmosphere at room temperature for 18 h. The mixture was filtered through Celite. The filtrate was concentrated and the crude product was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957064B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-81fc562003f548ffa06cdd3904f5e467 |
| Source note | uspto-grants-2015_02 |