HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(6-Phenylpyrazolo[1,5-a]pyrimidin-5-yl)benzaldehyde → HCID 178420107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(6-Phenylpyrazolo[1,5-a]pyrimidin-5-yl)benzaldehyde | HCID 86630665 | — |
| Reactant | HCID 178478275 | HCID 178478275 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178420107 | HCID 178420107 | — |
Reaction Steps
251.4 mg (0.84 mmol) 4-(6-phenylpyrazolo[1,5-a]pyrimidin-5-yl)benzaldehyde, a suspension in 10 mL DMF and 238 mg (1 mmol) 2-piperidine-4-yl-3H-imidazo[4,5-b]pyridine hydrochloride salt were stirred and treated as described in example 15.0. After stirring overnight at room temperature, the reaction mixture was worked up as described in example 15. After purification 90 mg of the desired product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957064B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-f16be0c1e4b840c5ba24471fb26e20e1 |
| Source note | uspto-grants-2015_02 |