HRID1851268
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
251.4 mg (0.84 mmol) 4-(6-phenylpyrazolo[1,5-a]pyrimidin-5-yl)benzaldehyde, a suspension in 10 mL DMF and 238 mg (1 mmol) 2-piperidine-4-yl-3H-imidazo[4,5-b]pyridine hydrochloride salt were stirred and treated as described in example 15.0. After stirring overnight at room temperature, the reaction mixture was worked up as described in example 15. After purification 90 mg of the desired product were obtained.
WORKUP
后处理
- additiontreated
- customAfter purification 90 mg of the desired product
- customwere obtained