HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5-Azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine → HCID 178482056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5-Azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine | HCID 68753485 | — |
| Reactant | 4-(2-Methyl-5-methylamino-6-phenyl-imidazo[1,2-a]pyrimidin-7-yl)benzaldehyde | HCID 86703055 | — |
| Product | HCID 178482056 | HCID 178482056 | — |
Reaction Steps
The compound is prepared in analogy to example 60. 416 mg 2-(5-Azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine×2HCl (60% pure) are reacted with 270 mg (0.79 mmol) 4-(2-methyl-5-methylamino-6-phenyl-imidazo[1,2-a]pyrimidin-7-yl)benzaldehyde to yield finally after HPLC purification 88.3 mg (20.7%) of the expected compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957064B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-472565b50d014178ad0612f563c5cdc9 |
| Source note | uspto-grants-2015_02 |