Trioctylamine → HCID 87299687, compound

HRID 1851735Notes

Reaction equation

HRID 1851735 reaction equation
[CH2:1]([N:9]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:26]([OH:31])(=[O:30])[C@H:27]([CH3:29])[OH:28]>>[C:26]([O-:31])(=[O:30])[CH:27]([CH3:29])[OH:28].[CH2:18]([NH+:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

3

Reactant 2

HCID 14227TrioctylamineHCID 107689L-Lactic Acid2×

Product 1

HCID 87299687HCID 87299687, compound

Procedure

In a mixing vessel, trioctylamine and L-lactic acid with an optical purity of 99% L-lactic acid was converted by heating to form trioctyl ammonium lactate. This was placed in a distillation vessel that was equipped with a reducing Liebig cooler and an Anschütz-Thiele distillation adaptor. Furthermore, 1 percent by mass (relative to lactic acid) dibutyltin oxide was placed as catalyst in the recipient vessel.

Workup

  1. temperatureby heating

Sources & evidence

ORD record
ord-82ee3154fae842c5a5492e746551b625
Source dataset
uspto-grants-2015_02
Patent number
US08957229B2

Reaction notes

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