HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 71075357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 71074601 | HCID 71074601 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71075357 | HCID 71075357 | — |
Reaction Steps
To the mixture of (S)—N-(1-(3-isopropylphenyl)ethyl)-2,3-dimethyl-1-((2′-sulfamoyl-[1,1′-biphenyl]-4-yl)methyl)-1H-indole-5-carboxamide (0.058 g, 0.1 mmol) and TEA (0.03 mL, 0.2 mmol) in DCM (0.5 mL) was slowly added acetyl chloride (0.009 g, 0.11 mmol). The mixture was stirred at room temperature for 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957093B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-8ccd641c13db4adba39c5405b4bba3dc |
| Source note | uspto-grants-2015_02 |