HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoyl chloride → HCID 67535862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | HCID 67534335 | HCID 67534335 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67535862 | HCID 67535862 | 60.2% |
Reaction Steps
A mixed solution of 300 mg of 4-(4-tert-butylphenyl)-2-(4-methoxyphenyl)pyrrole, 201 mg of 2-methoxybenzoylchloride, and 10 mL of toluene was heated at 120° C. for 6 hours under a nitrogen flow. After cooling to room temperature, evaporation was performed. After washing with 20 mL of ethanol and vacuum drying, 260 mg of 2-(2-methoxybenzoyl)-3-(4-tert-butylphenyl)-5-(4-methoxyphenyl)pyrrole was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962155B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-96f74cfd444e4fa381655dfea04cd7bb |
| Source note | uspto-grants-2015_02 |