HCID 1537019, compound → HCID 49872911, compound

Participants

Reaction Steps

3-Amino-6-phenylthieno[2,3-d]pyrimidin-4(3H)-one and 1-adamantaneacetyl chloride were reacted as described in Example 5 to provide the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.65-1.75 (m, 12H), 2.01-2.05 (m, 3H), 2.23 (s, 2H), 7.35-7.46 (m, 3H), 7.63-7.65 (m, 2H), 7.69 (s, 1H), 7.99 (s, 1H), 8.10 (s, 1H); MS (DCI/NH3) m/z 420 (M+H)+; Elemental Analysis: Calculated for C24H25N3O2S: C, 68.71; H, 6.01; N, 10.02. Found: C, 68.53; H, 5.65; N, 9.98.

Provenance & Evidence