HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 689541, compound → HCID 49872914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 689541 | HCID 689541 | — |
| Reactant | 1-Adamantaneacetyl chloride | HCID 2771882 | — |
| Product | HCID 49872914 | HCID 49872914 | — |
Reaction Steps
1-Adamantaneacetyl chloride and 3-amino-2,6-dimethylthieno[2,3-d]pyrimidin-4(3H)-one (Matrix) were processed using the method described in Example 42C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.54-1.76 (m, 12 H) 1.89-1.99 (m, 3 H) 2.04-2.18 (m, 2 H) 2.37 (s, 3 H) 2.5 (s, 3 H) 7.09 (s, 1 H) 10.83 (s, 1 H); MS (ESI+) m/z 372 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962639B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-6a3b607027f84d229f4017a5576054db |
| Source note | uspto-grants-2015_02 |