BRN 5958851 → HCID 49872915, compound

Participants

Reaction Steps

1-Adamantaneacetyl chloride and 3-amino-2-methyl-3,5,6,7,8,9-hexahydro-4H-cyclohepta[4,5]thieno[2,3-d]pyrimidin-4-one (Matrix) were processed using the method described in Example 42C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 1.49-1.76 (m, 15 H) 1.78-1.89 (m, 2 H) 1.91-2.00 (m, 3 H) 2.08 (d, J=15.0 Hz, 1 H) 2.16 (d, J=15.0 Hz, 1 H) 2.34 (s, 3 H) 2.84 (s, 2 H) 3.11-3.29 (m, 3 H) 10.76 (s, 1 H); MS (ESI+) m/z 426 (M+H)+.

Provenance & Evidence