HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromothiophene-2-carboxylic acid → HCID 67449611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromothiophene-2-carboxylic acid | HCID 2739688 | — |
| Reactant | 2-Fluoro-4-methoxyaniline | HCID 3756383 | — |
| Product | HCID 67449611 | HCID 67449611 | 90% |
Reaction Steps
Following Step 1 from General Procedure A, 3-bromothiophene-2-carboxylic acid (7.3 g, 35 mmol) was reacted with 2-fluoro-4-methoxyaniline (5.0 g, 35 mmol) to afford the desired product (10 g, 90%) as an orange solid: ESI MS m/z 331 [C12H1FNO2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-8acb834176a44fcfb9804d4e7935f2cd |
| Source note | uspto-grants-2015_02 |