huagongshe.com
HRID1853715

反应详情

EQUATION

反应方程式

HRID 1853715 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1Br
HCID67449139

未命名化合物

结构：C[C@@H](NC(=O)OC(C)(C)C)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1
HCID67467206

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1-c1ccc([C@@H](C)NC(=O)OC(C)(C)C)cc1
HCID86689472

未命名化合物

收率 47%

PROCEDURE

实验过程

Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (3.0 g, 9.7 mmol) was reacted with (R)-tert-butyl 1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethylcarbamate (5.0 g, 14 mmol) to afford the desired product (2.0 g, 47%) as a brown solid: ESI MS m/z 451 [C25H26N2O4S+H]+.