HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indazole → HCID 67448575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indazole | HCID 44119250 | — |
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Product | HCID 67448575 | HCID 67448575 | 31.5% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (100 mg, 0.32 mmol) was reacted with 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indazole (120 mg, 0.48 mmol) to afford the desired product (35 mg, 31%) as brown solid: ESI MS m/z 348 [C18H11N3O2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-abf369fa0e7348bf883fd44badfef054 |
| Source note | uspto-grants-2015_02 |