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HRID1853817

反应详情

EQUATION

反应方程式

HRID 1853817 的结构方程式

REACTANTS

反应物

2
结构：CB1OB(C)OB(C)O1
HCID574072

Trimethylboroxine

C3H9B3O3

结构：COc1cc(Br)c2[nH]c(=O)c3sccc3c2c1-c1ccc(C(C)NC(=O)OC(C)(C)C)cc1
HCID86689504

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C)c2[nH]c(=O)c3sccc3c2c1-c1ccc(C(C)NC(=O)OC(C)(C)C)cc1
HCID86689505

未命名化合物

收率 71.7%

PROCEDURE

实验过程

Following General Procedure J, tert-butyl 1-(4-(6-bromo-8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenyl)ethylcarbamate (32 mg, 0.060 mmol) was reacted with trimethylboroxine (8 mg, 0.060 mmol) to afford the desired product (20 mg, 61%) as a grey solid: ESI MS m/z 465 [C26H28N2O4S+H]+.