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HRID1853854

反应详情

EQUATION

反应方程式

HRID 1853854 的结构方程式

REACTANTS

反应物

2
结构：CB1OB(C)OB(C)O1
HCID574072

Trimethylboroxine

C3H9B3O3

结构：COc1cc(Br)c2[nH]c(=O)c3sccc3c2c1-c1ccc([C@H](C)CN(C)C(=O)OC(C)(C)C)cc1
HCID86689528

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C)c2[nH]c(=O)c3sccc3c2c1-c1ccc([C@H](C)CN(C)C(=O)OC(C)(C)C)cc1
HCID67447694

未命名化合物

收率 75%

PROCEDURE

实验过程

Following General Procedure J, (S)-tert-butyl 2-(4-(6-bromo-8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenyl)propyl(methyl)carbamate (150 mg, 0.269 mmol) was reacted with trimethyl boroxine (102 mg, 0.8 mmol) to afford the desired product (95 mg, 75%) as a brown solid: ESI MS m/z 493 [C28H32BrN2O4S+H]+.