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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1854685Generated: November 1, 2026

HCID 68551182, compound → HCID 68554115, compound

https://huagongshe.com/reaction/1854685

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68551182HCID 68551182—
ReactantHCID 68551771HCID 68551771—
SolventChloroform methanolHCID 21584188—
ProductHCID 68554115HCID 68554115—

Reaction Steps

The title compound was synthesized using the same procedure employed for Example 281, but with (1E,6E)-1-{4-[2-(tert-butoxycarbonylamino)acetylamino]phenyl}-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (18 mg, 39 μmol, synthesized in Example 268) as the starting material instead of (1E,6E)-1-[4-(tert-butoxycarbonylamino)phenyl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel chromatography (chloroform/methanol=95/5 to 80/20). The product was obtained as a solid (1.5 mg, 11%) having the following characteristic.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962674B2
Source datasetuspto-grants-2015_02
ORD IDord-a476c9f7b5334091a3f5e06d92fe56fa
Source noteuspto-grants-2015_02