HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68551182, compound → HCID 68554115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68551182 | HCID 68551182 | — |
| Reactant | HCID 68551771 | HCID 68551771 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 68554115 | HCID 68554115 | — |
Reaction Steps
The title compound was synthesized using the same procedure employed for Example 281, but with (1E,6E)-1-{4-[2-(tert-butoxycarbonylamino)acetylamino]phenyl}-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (18 mg, 39 μmol, synthesized in Example 268) as the starting material instead of (1E,6E)-1-[4-(tert-butoxycarbonylamino)phenyl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel chromatography (chloroform/methanol=95/5 to 80/20). The product was obtained as a solid (1.5 mg, 11%) having the following characteristic.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962674B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-a476c9f7b5334091a3f5e06d92fe56fa |
| Source note | uspto-grants-2015_02 |