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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1854686Generated: October 31, 2026

HCID 68551182, compound → HCID 68556127, compound

https://huagongshe.com/reaction/1854686

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68551182HCID 68551182—
ReactantHCID 68551589HCID 68551589—
SolventChloroform methanolHCID 21584188—
ProductHCID 68556127HCID 68556127—

Reaction Steps

The title compound was synthesized using the same procedure employed for Example 281, but with (1E,6E)-1-[1-(tert-butoxycarbony)-indolin-6-yl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (14 mg, 32 μmol, synthesized in Example 292) as the starting material instead of (1E,6E)-1-[4-(tert-butoxycarbonylamino)phenyl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel chromatography (chloroform/methanol=100/0 to 95/5). The product was obtained as a solid (1.4 mg, 13%) having the following characteristic.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962674B2
Source datasetuspto-grants-2015_02
ORD IDord-bbe8407fcbbb4cbb8f8f0915c46b1e9c
Source noteuspto-grants-2015_02