HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68551182, compound → HCID 68556127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68551182 | HCID 68551182 | — |
| Reactant | HCID 68551589 | HCID 68551589 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 68556127 | HCID 68556127 | — |
Reaction Steps
The title compound was synthesized using the same procedure employed for Example 281, but with (1E,6E)-1-[1-(tert-butoxycarbony)-indolin-6-yl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (14 mg, 32 μmol, synthesized in Example 292) as the starting material instead of (1E,6E)-1-[4-(tert-butoxycarbonylamino)phenyl]-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel chromatography (chloroform/methanol=100/0 to 95/5). The product was obtained as a solid (1.4 mg, 13%) having the following characteristic.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962674B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-bbe8407fcbbb4cbb8f8f0915c46b1e9c |
| Source note | uspto-grants-2015_02 |