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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1854707Generated: November 1, 2026

HCID 49806006, compound → HCID 68553421, compound

https://huagongshe.com/reaction/1854707

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 49806006HCID 49806006—
ReactantHCID 68549362HCID 68549362—
ProductHCID 68553421HCID 68553421—

Reaction Steps

The title compound was synthesized using the same procedure employed for Example 372, but with (1E,6E)-1-(9-ethyl-9H-carbazol-3-yl)-7-(3-hydroxy-4-methoxyphenyl)hepta-1,6-diene-3,5-dione (20 mg, 59 μmol, synthesized in Example 84) as the starting material instead of (1E,6E)-1-(4-dimethylaminophenyl)-7-(4-hydroxy-3-methoxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel column chromatography eluting with hexane/ethyl acetate=75/25 to 65/35. The product was obtained as a solid (13.1 mg, 65%) having the following characteristics.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962674B2
Source datasetuspto-grants-2015_02
ORD IDord-8359c52e6ff64698a9e34623c6f6fbe2
Source noteuspto-grants-2015_02