HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 49806006, compound → HCID 68553421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 49806006 | HCID 49806006 | — |
| Reactant | HCID 68549362 | HCID 68549362 | — |
| Product | HCID 68553421 | HCID 68553421 | — |
Reaction Steps
The title compound was synthesized using the same procedure employed for Example 372, but with (1E,6E)-1-(9-ethyl-9H-carbazol-3-yl)-7-(3-hydroxy-4-methoxyphenyl)hepta-1,6-diene-3,5-dione (20 mg, 59 μmol, synthesized in Example 84) as the starting material instead of (1E,6E)-1-(4-dimethylaminophenyl)-7-(4-hydroxy-3-methoxyphenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel column chromatography eluting with hexane/ethyl acetate=75/25 to 65/35. The product was obtained as a solid (13.1 mg, 65%) having the following characteristics.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962674B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-8359c52e6ff64698a9e34623c6f6fbe2 |
| Source note | uspto-grants-2015_02 |