HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4,6-dimethoxy-1,3,5-triazine → HCID 57345409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4,6-dimethoxy-1,3,5-triazine | HCID 18450 | — |
| Reactant | 7-Chloro-1,3-dihydro-2H-indol-2-one | HCID 3731010 | — |
| Product | HCID 57345409 | HCID 57345409 | — |
Reaction Steps
7-Chloro-1,3-dihydro-2H-indol-2-one (101.5 g) and 2-chloro-4,6-dimethoxy-1,3,5-triazine (152 g) are reacted analogously to Example 1 Variant A. This gives the title compound as solid in an HPLC purity of 99% area (181.9 g, 97% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962828B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-72ed9b1e450d42ea8e100ad9dff8a3cc |
| Source note | uspto-grants-2015_02 |