HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol, 2-chloro-5-(trifluoromethyl)- → HCID 53494183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol, 2-chloro-5-(trifluoromethyl)- | HCID 123498 | — |
| Reactant | Diisopropyl azodicarboxylate | HCID 5363146 | — |
| Reactant | HCID 86676671 | HCID 86676671 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53494183 | HCID 53494183 | — |
Reaction Steps
Compound 42 is prepared from 2-chloro-5-trifluoromethylphenol and intermediate 5d according to synthesis method 3 in toluene in the presence of DIAD, under the operating conditions described for example 8 (86% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962837B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-6e5eeab055cd47dd9bbe89efe1644e4f |
| Source note | uspto-grants-2015_02 |