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HRID1854817

反应详情

EQUATION

反应方程式

HRID 1854817 的结构方程式

REACTANTS

反应物

3
结构：Oc1cc(C(F)(F)F)ccc1Cl
HCID123498

Phenol, 2-chloro-5-(trifluoromethyl)-

C7H4ClF3O

结构：CC(C)OC(=O)/N=N/C(=O)OC(C)C
HCID5363146

Diisopropyl azodicarboxylate

C8H14N2O4

结构：OC1CCN(c2nccnn2)C1
HCID86676671

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)(F)c1ccc(Cl)c(OC2CCN(c3nccnn3)C2)c1
HCID53494183

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Compound 42 is prepared from 2-chloro-5-trifluoromethylphenol and intermediate 5d according to synthesis method 3 in toluene in the presence of DIAD, under the operating conditions described for example 8 (86% yield).