(2,6-Dichloropyridin-4-yl)methanol → HCID 57829746, compound

Participants

Reaction Steps

The title compound was prepared in analogous manner as described in example 1e) from 2,6-dichloropyridin-4-methanol (53 mg, 0.3 mmol) and 3-methoxy-4-(4-methyl-imidazol-1-yl)-phenylamine (61 mg, 0.3 mmol). The reaction was heated for 16 h to reflux. Obtained as a pale-yellow solid (25 mg, 24%) after column chromatography on silica gel using dichloromethane/methanol (9:1 v/v) as eluent.

Provenance & Evidence