HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylpyrimidine → HCID 86633625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylpyrimidine | HCID 79471 | — |
| Reactant | Sarcosine t-butyl ester hydrochloride | HCID 11252350 | — |
| Product | HCID 86633625 | HCID 86633625 | 52% |
Reaction Steps
Prepared in analogy to example 98a), using 2,4-dichloro-6-methylpyrimidine and sarcosine tert-butyl ester hydrochloride. The title compound was isolated as a slightly yellow oil in a yield of 52%. MS ISP (m/e): 272.2 & 274.0 (25 & 10) [(M+H)+]. 1H NMR (CDCl3, 300 MHz): δ (ppm)=6.23 (s broad, 1H), 4.21 (s broad, 2H), 3.10 (s broad, 3H), 2.36 (s, 3H), 1.46 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962834B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-41e8c918e0ba48d7a070faa2573db2fc |
| Source note | uspto-grants-2015_02 |