HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylpyrimidine → HCID 86633626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylpyrimidine | HCID 79471 | — |
| Reactant | Benzyl N-methylglycinate--hydrogen chloride (1/1) | HCID 18618415 | — |
| Product | HCID 86633626 | HCID 86633626 | 62% |
Reaction Steps
Prepared in analogy to example 98a), using 2,4-dichloro-6-methylpyrimidine and sarcosine-benzylester hydrochloride. The title compound was isolated as a slightly yellow oil in a yield of 62%. MS ISP (m/e): 306.1 & 308.2 (100 & 38) [(M+H)+]. 1H NMR (CDCl3, 300 MHz): δ (ppm)=7.40-7.35 (m, 5H), 6.23 (s broad, 1H), 5.19 (s, 2H), 4.39 (s broad, 2H), 3.11 (s broad, 3H), 2.36 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962834B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-c0dcb271383a47aa9add9084d2ee8c5a |
| Source note | uspto-grants-2015_02 |