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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1855537Generated: November 1, 2026

2-Chloro-4,6-dimethylpyrimidine → HCID 44192701, compound

https://huagongshe.com/reaction/1855537

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Chloro-4,6-dimethylpyrimidineHCID 20550—
ReactantHCID 20507215HCID 20507215—
ProductHCID 44192701HCID 44192701—

Reaction Steps

The title compound was prepared in analogy to example 62 from 4-(2-methyl-pyridin-4-yl)-phenylamine and 2-chloro-4,6-dimethylpyrimidine. Obtained as a yellowish solid (Yield=33%). MS ISP (m/e): 291.1 (100) [(M+H)+]. 1H NMR (DMSO-D6, 300 MHz): δ (ppm)=9.73 (s, 1H), 8.43 (d, 1H), 7.97 (d, 2H), 7.73 (d, 2H), 7.55 (s, 1H); 7.47 (d, 1H), 6.67 (s, 1H), 2.50 (s, 3H hidden in DMSO-peak), 2.34 (s, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962834B2
Source datasetuspto-grants-2015_02
ORD IDord-2edd761131514e2698e906d4cf67d159
Source noteuspto-grants-2015_02