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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1855538Generated: October 31, 2026

HCID 20507215, compound → HCID 44192793, compound

https://huagongshe.com/reaction/1855538

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 20507215HCID 20507215—
Reactant4-Benzyl-2-chloro-6-methyl-pyrimidineHCID 86633618—
ProductHCID 44192793HCID 44192793—

Reaction Steps

The title compound was prepared in analogy to example 62 from 4-(2-methyl-pyridin-4-yl)-phenylamine and 4-benzyl-2-chloro-6-methyl-pyrimidine (example 43a). Obtained as a yellowish solid (Yield=48%). MS ISP (m/e): 367.1 (100) [(M+H)+]. 1H NMR (DMSO-D6, 300 MHz): δ (ppm)=9.77 (s, 1H), 8.45 (d, 1H), 7.93 (d, 2H), 7.71 (d, 2H), 7.55 (s, 1H), 7.47 (d, 1H), 7.35-7.20 (m, 5H), 6.67 (s, 1H), 3.95 (s, 2H), 2.51 (s, 3H), 2.33 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962834B2
Source datasetuspto-grants-2015_02
ORD IDord-1a2fe6cda2d24134815559b58de8ff87
Source noteuspto-grants-2015_02