HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium cyanate → Sulbenox
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Reactant | 4,5,6,7-Tetrahydro-7-oxobenzo[b]thiophen-4-amine hydrochloride | HCID 23347795 | — |
| Solvent | Water | HCID 962 | — |
| Product | Sulbenox | HCID 65473 | — |
Reaction Steps
An aqueous solution of 4,5,6,7-tetrahydro-7-oxobenzo[b]thiophen-4-amine hydrochloride (1.01 g/5 ml water) is treated with 0.81 g of potassium cyanate in 2 ml of water at pH 6-7 to afford the title compound, which is collected and washed with water to afford 0.93 g, m.p. 241° C. to 242° C. dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216149 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-5cd6fc17efc6410fb75d3f7f28d37424 |
| Source note | uspto-grants-1980_08 |