Acetic Anhydride → HCID 12837908, compound

Participants

Reaction Steps

To a solution of 1.54 g. of N,N-dimethyl-2-(mercapto)acetamidine hydrochloride in 15 ml. of acetic acid was added 2 ml. of acetic anhydride, and the reaction mixture was heated at 55°-60° C. for 3 hours, after which it was concentrated in vacuo. The product was crystallized from ether, filtered, and air dried, then recrystallized from ethanol to yield 1.1 g., m.p. 162°-5°-163° C.

Provenance & Evidence