HRID1855800

反应详情

EQUATION

反应方程式

HRID 1855800 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

(E,E,E,E)-3,7-dimethyl-9-(2,4-dimethyl-3-furyl)-2,4,6,8-nonatetraenoic acid chloride (1.5 g.) was dissolved in a solution of methanol and sodium ethoxide (0.3 g.) and the resulting mixture was then concentrated to dryness to give sodium (E,E,E,E)-3,7-dimethyl-9-(2,4-dimethyl-3-furyl)-2,4,6,8-nonatetraenoate m.p.~280° with decomposition as an amorphous solid.

WORKUP

后处理

  1. concentrationthe resulting mixture was then concentrated to dryness