Ethanol → HCID 54075889, compound

HRID 1855846Notes

Reaction equation

HRID 1855846 reaction equation
[S:1]1[CH:5]=[CH:4][N:3]=[C:2]1[CH:6]=[CH:7][C:8]([OH:10])=[O:9].S(=O)(=O)(O)O.[CH2:16](O)[CH3:17]>>[S:1]1[CH:5]=[CH:4][N:3]=[C:2]1[CH:6]=[CH:7][C:8]([O:10][CH2:16][CH3:17])=[O:9]

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 534018492-Thiazoleacrylic acid

Product 1

HCID 54075889HCID 54075889, compound

Procedure

A solution of 2-thiazoleacrylic acid (26.76 g) and concentrated sulphuric acid (10 ml) in ethanol (150 ml) was refluxed for 18 hours. The solution was partially evaporated and dissolved in water. This solution was extracted with ether and the etheral extracts were evaporated to give ethyl 2-thiazoleacrylate.

Workup

  1. customThe solution was partially evaporated
  2. dissolutiondissolved in water
  3. extractionThis solution was extracted with ether
  4. customthe etheral extracts were evaporated

Sources & evidence

ORD record
ord-0f382b6700ff4b69984bf936cff911b3
Source dataset
uspto-grants-1980_08
Patent number
US04216318

Reaction notes

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