HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 2-thiazoleacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Thiazoleacrylic acid | HCID 53401849 | — |
| Product | Ethyl 2-thiazoleacrylate | HCID 54075889 | — |
Reaction Steps
A solution of 2-thiazoleacrylic acid (26.76 g) and concentrated sulphuric acid (10 ml) in ethanol (150 ml) was refluxed for 18 hours. The solution was partially evaporated and dissolved in water. This solution was extracted with ether and the etheral extracts were evaporated to give ethyl 2-thiazoleacrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216318 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-0f382b6700ff4b69984bf936cff911b3 |
| Source note | uspto-grants-1980_08 |