HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23347222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 23347223 | HCID 23347223 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 23347222 | HCID 23347222 | — |
Reaction Steps
To a solution of 10 parts of α-(4-biphenylyl)-α,α-bis[2-(diisopropylamino)ethyl]acetamide in 350 parts by volume of ether is added dropwise with stirring 2 molar equivalents of hydrochloric acid in isopropyl alcohol. The mixture is stirred for about 2 hours when the resulting salt is separated by filtration to afford α-(4-biphenylyl)-α,α-bis[2-(diisopropylamino)ethyl]acetamide dihydrochloride, as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04217306 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-1bbed574623f4bf1b292c9ce1317cd85 |
| Source note | uspto-grants-1980_08 |