HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12515297, compound → HCID 23346267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12515297 | HCID 12515297 | — |
| Reactant | Aluminiumhydride | HCID 21584524 | — |
| Reactant | HCID 23346235 | HCID 23346235 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23346267 | HCID 23346267 | — |
Reaction Steps
The product is prepared according to the procedure for the synthesis of 4-[(4-fluorophenyl)thio]-1,2,3,6-tetrahydropyridine hydrochloride by reducing 26.3 g of 4-[(4-chlorophenyl)thio]pyridine with aluminum hydride. The hydrochloride salt is generated in ether from the crude oil to afford a light tan powder, m.p. 174°-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218455 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-9ee0f930bd4b44a58a0b3bbdf5d980dc |
| Source note | uspto-grants-1980_08 |